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COURSE UNIT TITLECOURSE UNIT CODESEMESTERTHEORY + PRACTICE (Hour)ECTS
STRUCTURE ELUCIDATION IN DRUGS ECZ438 - 2 + 0 2

TYPE OF COURSE UNITElective Course
LEVEL OF COURSE UNITBachelor's Degree
YEAR OF STUDY-
SEMESTER-
NUMBER OF ECTS CREDITS ALLOCATED2
NAME OF LECTURER(S)Professor Osman Cihat Şafak
LEARNING OUTCOMES OF THE COURSE UNIT At the end of this course, the students;
1) Learns the basic spectral methods used in the structure of organic compounds.
2) Evaluates the spectra obtained from these methods
MODE OF DELIVERYFace to face
PRE-REQUISITES OF THE COURSENo
RECOMMENDED OPTIONAL PROGRAMME COMPONENTNone
COURSE DEFINITIONStructure determination of drug active ingredients. Introduction to spectroscopy and basic principles. Ultraviyolet and visible spectroscopy. Infrared spectroscopy, Nuclear magnetic resonance spectroscopy, Mass spectroscopy.
COURSE CONTENTS
WEEKTOPICS
1st Week Structure determination of drug active ingredients
2nd Week Introduction to spectroscopy and basic principles
3rd Week Introduction to spectroscopy and basic principles
4th Week Ultraviyolet and visible spectroscopy
5th Week Infrared spectroscopy
6th Week Infrared spectroscopy
7th Week Midterm exam
8th Week Nuclear magnetic resonance spectroscopy
9th Week Nuclear magnetic resonance spectroscopy
10th Week Nuclear magnetic resonance spectroscopy
11th Week Nuclear magnetic resonance spectroscopy
12th Week Nuclear magnetic resonance spectroscopy
13th Week Mass spectroscopy
14th Week Mass spectroscopy
RECOMENDED OR REQUIRED READING1. Silverstein, R.M., Webster F. X., `Spectrometric Identification of Organic Compounds?, New York, 2005.
2. Ergenç, N., `İlaçların Tanınması ve Kalitatif Tayini? İstanbul, 1989.
3. Skoog, D.A., West D.M., `Principle of Instrumental Analysis? Philadelphia, 1980.
4. Willard H. H., Merritt L. L., Dean J. A., Seettle, F. A., `Instrumental Method of Analysis?, Belmont California (1988).
5. Pouchert, C.J., Behnke, J., The Aldrich Library of 13C and 1H FT-NMR Spectra, Aldrich Chemical, Milwaukee (1992)
6. Balcı M., `Nucleer Magnetic Rezonans Spektroskopisi?, Ankara 2000.
7. Williams, D.H., Fleming, I., Spectroscopic Methods in Organic Chemistry, London (1995).
8. Crews P., Rodriguez J, Jaspars M., Organic Structure Analysis, New York (1998).
9. Shriner R L., Hermann C., Morrill TC., Curtin DY., Fuson RC, The Systematic Identification of Organic Compounds (1999).
10. Hesse, M., Meier, H., Zeeh, B., Spectroscopic Methods in Organic Chemistry, Thieme, Stuttgart (2008).
PLANNED LEARNING ACTIVITIES AND TEACHING METHODSLecture,Questions/Answers,Problem Solving,Discussion
ASSESSMENT METHODS AND CRITERIA
 QuantityPercentage(%)
Mid-term140
Total(%)40
Contribution of In-term Studies to Overall Grade(%)40
Contribution of Final Examination to Overall Grade(%)60
Total(%)100
ECTS WORKLOAD
Activities Number Hours Workload
Midterm exam111
Preparation for Quiz000
Individual or group work14114
Preparation for Final exam11010
Course hours14228
Preparation for Midterm exam155
Laboratory (including preparation)000
Final exam122
Homework000
Total Workload60
Total Workload / 302
ECTS Credits of the Course2
LANGUAGE OF INSTRUCTIONTurkish
WORK PLACEMENT(S)No
  

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